Liquid-Solid Separation
A research focus of the Institute of Particle Process Engineering of the University of Kaiserslautern is the development of methods for particle separation from liquids. The experimental and simulative experience in separation technology has been gathered for more than 10 years. It was conducted under the direction of Prof. Ripperger and will continue under his successor, Prof. Antonyuk.
The complementation of experiments with the modeling and simulation of multiphase flows is executed by numerical fluid mechanics (CFD) and CFD coupling with the discrete element method (DEM). With these methods, fundamental processes of the filtration can be investigated. Using CT-scans of the woven or nonwoven structure for the simulation can show the microflow and particle movement within the filter material.
The research of separation processes is supplemented by the classification of finest particles using dynamic filtration processes. As part of the priority programme SPP 2045: Highly specific and multidimensional fractionation of fine particle systems with technical relevance (MehrDimPart) of the DFG, the project Multidimensional fractionation of finely dispersed particles using cross-flow filtration with superimposed electric field is investigated at the Institute of Particle Process Engineering.
Team
Contact: Dr.-Ing. Kai Nikolaus
Research Areas
Research Projects
Development of membrane-woven-composite filtermedia for continuous cake filtration without gas throughput (21685 N)
August 1, 2021
Contact: Nikolai Benz
Funding: AiF
Highly specific multidimensional fractionation of technical fine particle systems
September 1, 2020
Contact: Simon Paas
Funding: AiF
Development of a method for the design of industrial filtration process based on experimental laboratory tests with analytical photofiltration centrifuges
August 7, 2020
Contact: Simon Paas
Funding: AiF ZIM
AiF-Project „Investigation of the flow and structure mechanical behavior of filter media and filter elements in operation“ (20859 N)
October 1, 2019
Contact: Vanessa Puderbach
Funding: AiF
High-Efficient seperation of particle-laden gas flows in a turbulent centrifugal field considerung particle agglomeration
August 20, 2019
Contact: Dzmitry Misiulia
Funding: AvH
Completed Research Projects
Successful completion of iGF project 20859N "Investigation of the flow and structure mechanical behavior of filter media and filter elements in operation".
October 1, 2019
Contact: Vanessa Puderbach
Funding: AiF
Multidimensional fractionation of finely dispersed particles using the cross-flow filtration with superimposed electric field
September 1, 2017
Contact: Philipp Lösch
Funding: DFG
Entwicklung eines automatisch rückspülbaren Kunststofffilters mit Eignung zur Aufreinigung saurer Prozesslösungen von Beizbädern
March 31, 2017
Funding: AIF-ZIM
Entwicklung eines Recyclingverfahrens zur Rückgewinnung von Kupfer und Salzsäure aus Goldscheideprozessen
March 31, 2017
Funding: AIF-ZIM
Experimentelle und numerische Untersuchungen zum Abscheideverhalten neuer und gealterter Elektretfilter
September 1, 2016
Contact: Maximilian Kerner, Kilian Schmidt
Funding: AiF
Classification of finest particles using crossflow filtration
September 1, 2016
Contact: Philipp Lösch
Funding: AiF
Berechnung der Kuchenfiltration in Fließschemasimulationen mit numerischen Verfahren
August 31, 2016
Contact: Frank Feser
Funding: AiF
Filtration von Suspensionen mittels autodynamischer hochfrequenter Rückspülung
October 31, 2014
Contact: Denis Goldnik, Kai Nikolaus
Funding: AiF
Methode zur Auslegung von optimierten Tiefenfiltern
October 31, 2014
Contact: Lars Peterson
Funding: AiF-IGF
Recent Publications
Puderbach V., Kirsch R., Antonyuk S.: Experimental Characterization of the Mechanical Properties of Filter Media in Solid–Liquid Filtration Processes. Materials (2024) 17(18):4578. https://doi.org/10.3390/ma17184578
Benz, N., Krull, F., Nikolaus, K., Antonyuk, S.: Membrane-fabric composite filter media for continuous cake filtration without gas throughput using paste dot coating with adhesive, Membranes 13 (9) (2023) 801, https://doi.org/10.3390/membranes13090801
Hesse, R., Lösch, P., Antonyuk, S.: CFD-DEM analysis of internal packing structure and pressure characteristics in compressible filter cakes using a novel elastic-plastic contact model, Advanced Powder Technology 34 (2023) 104062, https://doi.org/10.1016/j.apt.2023.104062
Weirich, M., Antonyuk, S.: Monitoring of particulate fouling potential of feed water with spectroscopic measurements, Membranes (2023) 13(7):664, https://doi.org/10.3390/membranes13070664
Kleffner, Ch., Braun, G., Ripperger, S., Antonyuk, S.: Methods for using direct numerical simulation for the investigation and optimization of the flow in spacerfilled channels of membrane elements, F&S Filtrieren und Separieren 03 (2023)
Benz, N., Lösch, P., Antonyuk, S.: Influence of the Measurement Resolution on the Filtration Analysis: An Improved Test Setup According to VDI 2762 Guideline. Processes 2023, 11, 299. doi.org/10.3390/pr11020299
Lösch, P.: Methoden zur diskontinuierlichen und kontinuierlichen hydrodynamischen Klassierung feinster Partikeln in einer Querströmung. Dissertation, Schriftenreihe des Lehrstuhls für Mechanische Verfahrenstechnik der TU Kaiserslautern, (2021) Band 25, ISBN 978-3-95974-169-9
Kleffner, C., Braun, G., Antonyuk S.: High-pressure reverse osmosis for industrial water recycling: Permeate-sided pressure drop as performance-limiting factor, Chemie Ingenieur Technik (2021), https://doi.org/10.1002/cite.202100021
Puderbach, V.; Schmidt, K.; Antonyuk, S.: A Coupled CFD-DEM Model for Resolved Simulation of Filter Cake Formation during Solid-Liquid Separation. In: Processes 9 (5), 2021. https://doi.org/10.3390/pr9050826.
P. Lösch, K. Nikolaus, S. Antonyuk, Fractionating of Finest Particles Using Cross-flow Separation with Superimposed Electric Field, Separation and Purification Technology (2021) 117820. https://doi.org/10.1016/j.seppur.2020.117820
Deshpande, R., Antonyuk, S., Iliev, O.: DEM-CFD study of the filter cake formation process formed due to non-spherical particles, Particuology (2020), https://doi.org/10.1016/j.partic.2020.01.00
Hund, D., Lösch, P., Kerner, M., Ripperger, S, and S. Antonyuk: CFD-DEM study of bridging mechanisms at the static solid-liquid surface filtration, Powder Technology 361 (2020), 600-609 https://doi.org/10.1016/j.powtec.2019.11.072
Deshpande, R.: Investigation of the Filter Cake Formation Process using DEM-CFD Simulation with Experimentally Calibrated Parameters. Stuttgart: Fraunhofer Verlag, 154 S., (2019), ISBN: 978-3-8396-1519-5
Barth, J,: Methode zur Auslegung von Apparaten und Maschinen zur dynamischen Oberflächenfiltration, Fortschritt-Berichte ; Band 22; Technische Universität Kaiserslautern, Lehrstuhl für Mechanische Verfahrenstechnik (2019), ISBN: 978-3-95974-122-4
Steinle, J. P.: Entwicklung und Untersuchung getauchter Niederdruck-Spiralwickel-Elemente zur Ultrafiltration, Fortschritt-Berichte, Band 21, Technische Universität Kaiserslautern, Lehrstuhl für Mechanische Verfahrenstechnik (2019), ISBN: 978-3-95974-119-4
Hund, D.: Methoden zur Simulation der Kuchenfiltration, Fortschritt-Berichte, Band 19, Technische Universität Kaiserslautern, MVT, Lehrstuhl für Mechanische Verfahrenstechnik (2019), ISBN: 978-3-95974-111-8
Lösch, P., Nikolaus, K., Antonyuk, S.: Classification of fine particles using the hydrodynamic forces in the boundary layer of a membrane, Chemie Ingenieur Technik 91 (2019) 11, 1656-1662. https://doi.org/10.1002/cite.201900052
Deshpande, R., Antonyuk, S., Iliev, O.: Study of the filter cake formed due to the sedimentation of mono and bi-dispersed particles using DEM-CFD simulations, AIChE Journal 65, (2019) 4, 1294-1303 https://doi.org/10.1002/aic.16529
Ripperger, S.; Schwarz, N.; Antonyuk, S.: Scaling und Fouling Observation bei Membrananlagen. Filtrieren und Separieren 33 (6) (2019), pp. 386–391
Kleffner, C., Braun, G., Antonyuk, S: Influence of membrane intrusion on permeate-sided pressure drop during high-pressure reverse osmosis, Chemie Ingeniuer Technik 91 (2019) 4, 1-13 https://doi.org/10.1002/cite.201800104
Deshpande, R.; Antonyuk, S.; Iliev, O. (2019): Study of the Filter Cake Formed due to the Sedimentation of Mono and Bi-dispersed Particles Using DEM-CFD Simulations. In AIChE J (accepted). https://doi.org/10.1002/aic.16529
Barth, J.; Koras, T.; Antonyuk, S.; Ripperger, S.: Metallrückgewinnung und Säureaufbereitung unter Nutzung von Membranverfahren. In Filtrieren und Separieren 32 (4) (2018), pp. 264–269
Barth, J.; Ripperger, S. (2018a): Methode zur Auslegung und Optimierung von dynamischen Oberflächenfiltern – Teil 1: Auslegung hinsichtlich des spezifischen Filtratstroms. In Filtrieren und Separieren 32 (1), pp. 12–17.
Barth, J.; Ripperger, S. (2018b): Methode zur Auslegung und Optimierung von dynamischen Oberflächenfiltern – Teil 2: Optimierung hinsichtlich des spezifischen Energiebedarfs. In Filtrieren und Separieren 32 (3), pp. 185–189.
Hund, D.; Schmidt, K.; Ripperger, S.; Antonyuk, S. (2018): Direct numerical simulation of cake formation during filtration with woven fabrics. In Chemical Engineering Research and Design 139, pp. 26–33. https://doi.org/10.1016/j.cherd.2018.09.023
Laboratory Equipment
Measurement of the mechanical solid-liquid-separation by cake filtration
Setup according VDI 2762
Measurement of compressible filter cakes
Inhouse developed compression-permeability cell
Cross-flow filtration
Multiple experimental setups for tubular or flow-channel membranes. Superimposed electric field or backflush analysis.
Rotating disc filters
Single or multi-shift filters
Filter Media analysis
SEM (Phenom G2 Pro)
Computer-Micro-Tomograph (µ-CT, Werth)
Measurement of the pore size distribution from porous media(Porometer Model PSM 165, Topas GmbH))
Zeta-potential of bulk and woven materials (IKA, Anton-Paar)
Contact angle measuring device
Measurement of wetting properties from surfaces contacted by aerosol droplets
High speed cameras
Measurement of particle / droplet trajectories
Particle size measurement from 1 nm to 3 mm
static light scattering (Horiba LA 950, Retsch)
dynamic light scattering (Zetasizer Nano ZS, Malvern)
particle counter (Abakus, Markus Klotz GmbH)
containment sensors (Hydac)
Particle property measurement
Measurement of bulk porosity (Ultra-Pycnometer Model 1000T, Quantachrome)
Measurement of the inner surface from porous media (BET-Analysis Model Nova 200e, Quantachrome)
Measurement of the zeta-potential (Zetasizer Nano ZS, Malvern & PCD-05, Mütek)
Analytical centrifuge (LUMiSizer, LUM GmbH)
Dispersion Analysis
Simulation Tools
CFD Simulation
4 ways coupled CFD-DEM and resolved Lattice-Boltzmann-DEM
Coupled CFD-DEM