3D microstructure: • Porosity, defects, cracks • Grain size and shape • Packing structure • Mixing, segregation
Aggregates, coatings: • Coating thickness • Microstructure, porosity • Distribution of components/binder
• Particle/agglomerate breakage behavior | Micro Computed Tomography (Werth Messtechnik GmbH) with a dual X-ray tube system: • nano transmission tube (160 kV), minimum voxel size of 500 nm • micro transmission tube (240 kV), minimum voxel size of 1.5 µm • high-resolution large-area detector (400x400 mm/ 4000x4000 px)
In situ compression test cell (Deben): • force and displacement measurement during uniaxial compression/ tension of a sample (single particles, packing, layer, coating) • CT imaging of the microstructure during stressing (consolidation, crack initiation and propagation) |